Zero-shot Autonomous Microscopy for Scalable and Intelligent Characterization of 2D Materials

Characterization of atomic-scale materials traditionally requires human experts with months to years of specialized training. Even for trained human operators, accurate and reliable characterization remains challenging when examining newly discovered materials such as two-dimensional (2D) structures. This bottleneck drives demand for fully autonomous experimentation systems capable of comprehending research objectives without requiring large training datasets. In this work, we present ATOMIC (Autonomous Technology for Optical Microscopy & Intelligent Characterization), an end-to-end framework that integrates foundation models to enable fully autonomous, zero-shot characterization of 2D materials. Our system integrates the vision foundation model (i.e., Segment Anything Model), large language models (i.e., ChatGPT), unsupervised clustering, and topological analysis to automate microscope control, sample scanning, image segmentation, and intelligent analysis through prompt engineering, eliminating the need for additional training. When analyzing typical MoS2 samples, our approach achieves 99.7% segmentation accuracy for single layer identification, which is equivalent to that of human experts. In addition, the integrated model is able to detect grain boundary slits that are challenging to identify with human eyes. Furthermore, the system retains robust accuracy despite variable conditions including defocus, color temperature fluctuations, and exposure variations. It is applicable to a broad spectrum of common 2D materials-including graphene, MoS2, WSe2, SnSe-regardless of whether they were fabricated via chemical vapor deposition or mechanical exfoliation. This work represents the implementation of foundation models to achieve autonomous analysis, establishing a scalable and data-efficient characterization paradigm that fundamentally transforms the approach to nanoscale materials research.

A microwave photonic prototype for concurrent radar detection and spectrum sensing over an 8 to 40 GHz bandwidth

In this work, a microwave photonic prototype for concurrent radar detection and spectrum sensing is proposed, designed, built, and investigated. A direct digital synthesizer and an analog electronic circuit are integrated to generate an intermediate frequency (IF) linearly frequency-modulated (LFM) signal with a tunable center frequency from 2.5 to 9.5 GHz and an instantaneous bandwidth of 1 GHz. The IF LFM signal is converted to the optical domain via an intensity modulator and then filtered by a fiber Bragg grating (FBG) to generate only two 2nd-order optical LFM sidebands. In radar detection, the two optical LFM sidebands beat with each other to generate a frequency-and-bandwidth-quadrupled LFM signal, which is used for ranging, radial velocity measurement, and imaging. By changing the center frequency of the IF LFM signal, the radar function can be operated within 8 to 40 GHz. In spectrum sensing, one 2nd-order optical LFM sideband is selected by another FBG, which then works in conjunction with the stimulated Brillouin scattering gain spectrum to map the frequency of the signal under test to time with an instantaneous measurement bandwidth of 2 GHz. By using a frequency shift module to adjust the pump frequency, the frequency measurement range can be adjusted from 0 to 40 GHz. The prototype is comprehensively studied and tested, which is capable of achieving a range resolution of 3.75 cm, a range error of less than $\pm$ 2 cm, a radial velocity error within $\pm$ 1 cm/s, delivering clear imaging of multiple small targets, and maintaining a frequency measurement error of less than $\pm$ 7 MHz and a frequency resolution of better than 20 MHz.