Abstract:Smart cities play a vital role in the growth of a nation. In recent years, several countries have made huge investments in developing smart cities to offer sustainable living. However, there are some challenges to overcome in smart city development, such as traffic and transportation man-agement, energy and water distribution and management, air quality and waste management monitoring, etc. The capabilities of the Internet of Things (IoT) and artificial intelligence (AI) can help to achieve some goals of smart cities, and there are proven examples from some cities like Singapore, Copenhagen, etc. However, the adoption of AI and the IoT in developing countries has some challenges. The analysis of challenges hindering the adoption of AI and the IoT are very limited. This study aims to fill this research gap by analyzing the causal relationships among the challenges in smart city development, and contains several parts that conclude the previous scholars work, as well as independent research and investigation, such as data collection and analysis based on DEMATEL. In this paper, we have reviewed the literature to extract key chal-lenges for the adoption of AI and the IoT. These helped us to proceed with the investigation and analyze the adoption status. Therefore, using the PRISMA method, 10 challenges were identified from the literature review. Subsequently, determination of the causal inter-relationships among the key challenges based on expert opinions using DEMATEL is performed. This study explored the driving and dependent power of the challenges, and causal relationships between the barriers were established.